A series of 1-[ω-[(arylamino)carbonyl]alkyl]-4-(benzocycloalkyl)piperazines I (R = F, CF3, Me, Ph, OMe, m = 1-3, n = 2, 3) was prepared either by reacting the precursor 4-[ω-[(arylamino)carbonyl]alkyl]piperazine II with 1-chlorobenzocycloalkanes III (Procedure A) or by reacting the N-aryl-ω-chloroalkananamides 4-RC6H4NHCO(CH2)nX (X = Br, Cl) with the 4-(benzocycloalkyl)piperazines IV (Procedure B). The best yields were obtained using procedure A.